有机化学实验（英汉双语教材）
作 者： 陈彪，魏永慧 编
出版时间：2013
丛编项： 英汉双语教材
内容简介
《高等学校“十二五”规划教材：有机化学实验（英汉双语教材）》是编者在总结多年来有机化学实验的教学经验及近年来实施双语教学实践的基础上，参考了国内外出版的同类教材，采用英汉两种语言，编写的与有机化学双语课程配套使用的《有机化学实验》教材。《高等学校“十二五”规划教材：有机化学实验（英汉双语教材）》包括：有机化学实验的一般知识，有机化学实验的基础知识和基本操作，有机化学综合实验（包括合成及分离提取两大部分），附录及参考文献。《高等学校“十二五”规划教材：有机化学实验（英汉双语教材）》可使学生在掌握有机化学实验基本原理、基本技能的同时，提高英语实际应用能力和水平，适用于化学、医学、药学及相关专业的学生使用，也可作为有机化学及相关专业硕士研究生的实验参考书。
目录
Chapter 1Introduction of Experimental
Organic Chemistry1
1?1Basic Rules for the Organic
Chemistry Lab1
1?2Common Lab Equipment and
Apparatus2
1?3General Lab Safety7
1?4Disposal of Lab Waste9
1?5Common Organic Solvents9
1?6Experimental Preview Record and
Laboratory Report13
1?7Chemical Literature14
Reference15
Chapter 2Basic Experimental
Techniques17
2?1Heating and Cooling17
2?2Drying and Drying Agent17
2?3Filtration19
2?4Solvent Extraction and Solution
Washing21
2?5The Purification and Separation of
Liquid Organic Substances24
2?6The Purification and Separation of
Solid Organic Substances32
2?7Chromatographic Techniques38
2?8The Determination of the Physical Constant
of Organic Compound47
Chapter 3Comprehensive Experiment56
Part 1Synthesis56
3?1Synthesis of Cyclohexene56
3?2Synthesis of Ethyl Bromide57
3?3Synthesis of 2?chlorobutane
(sec?butyl chloride)59
3?4Synthesis of diethyl ether61
3?5Synthesis of Phenetole
(ethyl phenolate)62
3?6Synthesis of Benzoic Acid and
Benzyl Alcohol63
3?7Synthesis of Acetophenone65
3?8Synthesis of Benzophenone (Friedel?
Crafts acylation method)67
3?9Synthesis of Cyclohexanone69
3?10Synthesis of Adipic Acid71
3?11Synthesis of Benzoic Acid73
3?12Synthesis of Cinnamic Acid74
3?13Synthesis of Ethyl Acetate76
3?14Synthesis of Isoamyl Acetate
(banana oil)78
3?15Synthesis of Acetylsalicylic
Acid (aspirin)79
3?16Synthesis of Methyl Salicylate
(oil of wintergreen)81
3?17Synthesis of Ethyl Acetoacetate83
3?18Synthesis of Acetanilide84
3?19Synthesis of p?toluidine86
3?20Synthesis of Anthranilic Acid
(2?aminobenzoic acid)88
3?21Synthesis of Phenoxyacetic Acid90
3?22Synthesis of Methyl Orange92
3?23Synthesis of Benzocaine94
3?24Synthesis of N?acetyl?p?toluidine96
3?25Synthesis of Benzoin96
3?26Synthesis of 2?Nitroresorcinol98
3?27Synthesis of Quinoline100
3?28Synthesis of Nikethamide103
3?29The Reduction of Camphor104
3?30Synthesis of 3?(2,5?xylyloxyl)
Propyl Chloride and Monitoration of
Reaction Process106
Part 2Extraction and Separation107
3?31The Recrystallization of Benzoic
Acid107
3?32Extraction and Purification of
Nicotine109
3?33Isolation of Caffeine From
Tea Leave110
3?34Isolation of Effective Components
from the Citrus112
3?35Isolation of Benberine from Coptis
chinensis Franch114
3?36Paper Chromatography of Amino
Acid115
3?37Paper Electrophoresis of Amino
Acid117
3?38Separation of Green Leaf Pigments
by TLC119
Chapter 4Appendix121
4?1Experiments from the Literature121
4?2List of the Elements with Their
Symbols and Atomic Masses123
4?3Main Families of Organic
Compounds126
4?4Boling Point and Density of Some
Common Organic Reagents126
第1章有机化学实验基础知识127
1?1有机化学实验的基本规则127
1?2常用的玻璃仪器和实验装置127
1?3有机化学实验的安全知识129
1?4有机化学实验废物的处置130
1?5常用有机溶剂及纯化130
1?6实验预习记录和实验报告134
1?7有机化学的文献资料134
第2章有机化学实验基本操作136
2?1加热和冷却136
2?2干燥与干燥剂136
2?3过滤137
2?4萃取和洗涤139
2?5液体有机化合物的分离与纯化142
2?6固体有机化合物的提纯147
2?7色谱法151
2?8有机化合物物理常数的测定156
第3章综合实验163
第一部分制备163
3?1环己烯的制备163
3?2溴乙烷的制备164
3?32?氯丁烷的制备165
3?4乙醚的制备166
3?5苯乙醚的制备167
3?6苯甲醇和苯甲酸的制备168
3?7苯乙酮的制备169
3?8二苯甲酮（酰基化法）的制备171
3?9环己酮的制备172
3?10己二酸的制备173
3?11苯甲酸的制备175
3?12肉桂酸的制备176
3?13乙酸乙酯的制备177
3?14乙酸异戊酯的制备（香蕉油）178
3?15乙酰水杨酸的制备（阿司匹林）180
3?16水杨酸甲酯的制备（冬青油）181
3?17乙酰乙酸乙酯的制备182
3?18乙酰苯胺的制备183
3?19对甲苯胺的合成184
3?20邻氨基苯甲酸的合成185
3?21苯氧乙酸的制备187
3?22甲基橙的制备189
3?23苯佐卡因的制备190
3?24对甲基?N?乙酰苯胺的合成192
3?25安息香的合成192
3?262?硝基雷琐酚的制备194
3?27喹啉的制备195
3?28尼可刹米的制备197
3?29樟脑的还原反应199
3?30降血脂药吉非贝齐中间体3?（2，5?二
甲基苯氧基）?1?氯丙烷的制备200
第二部分提取、分离与鉴定201
3?31苯甲酸的提纯201
3?32烟碱的提取与鉴定202
3?33从茶叶中提取咖啡因203
3?34橘皮中有效成分的提取、分离
与鉴定205
3?35黄连中黄连素的提取及鉴定206
3?36纸色谱分离鉴定氨基酸208
3?37纸上电泳分离鉴定氨基酸209
3?38薄层色谱法分离叶绿素210
参考文献212
